Wastewater Case Studies 2
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Case Studies: Wastewater 2

Alenco
E. I. DuPont De Nemours & Company

E. I. du Pont de Nemours & Company-Adiponitrile

H-R Industries

IBM

International Garment Processors

International Paper

Jones Blair Company

Kelly Air Force Base: Chromates

Kelly Air Force Base

Lone Star Radiator Company, Inc.

Murdock Engineering Company: Hexavalent Chromium

Texas Eastman: Organic Waste

Texas Eastman: Waste Oil Burning

Texas Instruments

Witco, Inc.: Three Projects

 

 

 

 


Alenco

arenco1.93

1. GENERAL INFORMATION

 

Location: Bryan

Number of Employees: 850

Industry: Aluminum Products

Waste Reduced: Wastewater, Chromium

Process: Electroplating

Contact Person: Chuck Fontaine, (409) 779-7770

 

2. DESCRIPTION OF PROJECT

 

ALENCO extrudes and paints aluminum for the building products industry. The extrusions were conversion coated with hexavalent chromium prior to painting to enhance the adhesion between the coating and the aluminum. In 1991, ALENCO made a corporate decision to eliminate chromium from its operation. After extensive testing, a zirconic acid system was selected. The equipment was modified and additional equipment installed in December 1991. On-line testing began in January 1992. Production began in June 1992. To date, in excess of 45 million pounds of aluminum have been successfully coated with this system.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The technology of replacing chromium with zirconium is not new. Some formulation modifications were necessary to improve flow and provide more uniform drying. Other minor application changes were also required. The major factor in the success of this project was the corporate decision to make it happen.

 

4. ENVIRONMENTAL BENEFIT

 

The process eliminated the use of hexavalent chromium that had to be converted to trivalent chromium to be acceptable for disposal. The conversion was costly and produced over 160 cubic yards of waste to be landfilled. The potential liabilities were enormous. The change to the zirconic acid system eliminated the use of chromium, its associated waste streams and its liabilities.

 

5. COST SAVINGS/BENEFIT

 

Modifications to the existing system cost $60,000. Disposal cost savings for the first year were $60,000. Return on investment was one year. With constantly increasing disposal costs, the economic benefits are clear.

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E. I. DuPont De Nemours & Company

dupont4.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: La Porte

Number of Employees: 1,070

Industry: Herbicide

Waste Reduced: Wastewater

Process: Product Recovery

Contact Person: Angela T. Jenkins-Kirby, (713) 470-3253

 

2. DESCRIPTION OF PROJECT

 

A Heinkel centrifuge unit is being installed to decrease the quantity of uracil herbicide carried into the filtrate waste stream. The stream is treated by the site's permitted biotreatment system. In addition to the reclamation of the herbicides previously lost to the wastewater treatment system, a large percentage of the uracil herbicide unit's discharge of water will be recycled into the process, thereby eliminating a portion of fresh make-up water.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

Although centrifugal filtration has often been used to improve marketable products, its sole purpose in this project was to improve waste stream characteristics so the site would be able to comply with new regulatory requirements on herbicides, effective December 1994.

 

4. ENVIRONMENTAL BENEFIT

 

This project has reduced one uracil herbicide in the waste stream by 8,900 lb/yr. It is expected to reduce the quantity of another uracil herbicide in the waste stream by 119,000 lb/yr. Total organic carbon (TOC) loadings to the site's wastewater treatment plant from uracil herbicide production will be reduced by 41 % overall. Additionally, hydraulic loadings will be reduced 51%, and EPCRA emissions/wastes and uracil herbicides waste will also be reduced.

 

5. COST SAVINGS/BENEFIT

 

Savings are estimated at $40,000 per year due to yield improvements and reduced treatment costs, alone. The substantial reductions of uracil herbicides in the wastewater provided additional time to evaluate other alternatives needed to meet even more stringent regulations, effective 1997. They also allowed the delay of $4MM in capital expenditures for "end of pipe" treatment. Recent evaluations indicate a possibility to avoid $3MM of that originally contemplated "end of pipe" treatment expense due to better source reduction and more economical treament alternatives.

 

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E. I. du Pont de Nemours & Company-Adiponitrile

dupont7.92

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Orange, Orange County

Number of Employees: 2,000

Industry: Adiponitrile

Waste Reduced: Wastewater

Process: Shut Off Seal Flush Water

Contact Person: R. H. Batig

 

 

2. DESCRIPTION OF PROJECT

 

In the Adiponitrile Production Unit 36 pumps are used to pump either sumps or process equipment to the waste treatment facilities prior to deepwelling the aqueous waste. These pumps are equipped with a single mechanical seal and a throttle bushing. The estimated 3 gpm of spent seal flush water mixes directly with the pumpage, and adds to the waste load.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

To minimize expenditure and still provide a flushed seal, we installed a solenoid valve connected to pump motor controls which allows seal flush water to flow only when the pump is running. In addition we installed a rotometer for flush water flow measurement and control and thus can reduce the amount of waste generated.

 

4. ENVIRONMENTAL BENEFIT

 

Estimated waste water reduction is approximately 57MM gal/yr.

 

5. COST SAVINGS

 

Payback period for these modifications is under a year.

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H-R Industries

h-rindus.92

1. GENERAL INFORMATION

 

Location: Richardson

Number of Employees: 100

Industry: Electronics

Waste Reduced: Sludge, Tin/Lead

Process: Process Change, Soldering

Contact: Gary C. Roper, (214) 301-6600

 

2. PROJECT DESCRIPTION

 

Over the period of a year our product mix changes from producing 90% solder coated circuits to producing 80% solder mask over bare copper (SMOBC) circuits. In both processes tin lead was plated over the circuits to act as an etch resist. The tin lead is stripped off after etch on SMOBC product. The change in product mix increased the lead in the influent to waste treatment from 1 mg/1 to 35 mg/1 in a 50 gpm system. This is an increase of approximately 2,300 kg per year of lead added to our sludge. The etch resist plating was changed to acid tin for SMOBC boards reducing the influent to waste treatment to below original levels.

 

3. TECHNOLOGY APPLICATION

 

Electroplating tin, etching the base copper, striping the tin, masking over the copper circuits, and applying solder by hot air solder level to only the holes allows for less lead on the finished product and no ionic forms of lead in high concentrations in the production process.

 

4. ENVIRONMENTAL BENEFIT

 

The process change reduced the amount of lead in the waste water treatment sludge by 5,000 pounds per year just from rinse water. This reduced sludge generation by 52 drums per year. The 3,300 gallons of stripping solution which averaged over 10 g/1 was condensed and disposed of off-site. Now that the stripping solution no longer contains lead it is treated in house with other corrosive solutions, reducing the lead waste by 275 pounds per year and reducing liability

 

5. COST SAVINGS/BENEFIT

 

The savings in reduced disposal cost is $14,000 per year. The project cost was $20,000 thus pay back will be 1.5 years.

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IBM

ibm2.95

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Austin

Number of Employees: 7,000

Industry: Electronics

Waste Reduced: Water Reuse

Process: Water Cleaning Operations & Rinse Water

Contact Person: Jeff Erb (512) 838-6978

 

2. DESCRIPTION OF PROJECT

 

IBM produces multilayered circuit boards in its north Austin plant. Aqueous baths and rinse water are processed at a pretreatment facility where acidity is neutralized and dissolved copper is removed prior to discharge into the sanitary sewer for further treatment at a POTW (Publicly Owned Treatment Works). In 1994 147,000,000 gallons were treated. In an effort to reduce water consumption, a team of environmental, facility and manufacturing engineers was assembled to find uses for the relatively clean wastewater from selected operations. The most likely destination for the water was the cooling tower, which used 101,000,000 gallons in 1994.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The team determined that there were several mechanical cleaning operations in the manufacturing process which required large quantities of fresh water for rinsing. The cleanliness of the product after these cleaning steps was critical to the next manufacturing step. The rinse water from these processes contained little or no dissolved metals.

 

In 1995, IBM segregated used rinse water from the wastewater used in manufacturing operations that contained dissolved metals and required further treatment. The used rinse water, on the other hand, contained only traces of dissolved metals and already met sanitary sewer pretreatment standards. This segregated rinse water was collected and fed into the cooling towers, replacing a portion of the fresh water being fed to the cooling tower.

 

4. ENVIRONMENTAL BENEFIT

 

Water collected for reuse has averaged 3,350,000 gallons per month for the first three months of operation.

 

  1. COST SAVINGS/BENEFITS

 

The project cost approximately $85,000 to implement. At the rate of 3,350,000 gallons a month the annual cost savings on the project will be $210,000.

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International Garment Processors

igp1.94

1. GENERAL INFORMATION

 

Location: El Paso

Number of Employees: 750

Industry: Industrial Laundry

Waste Reduced: Wastewater

Process: Water Reuse

Contact Person: George Essenberg, (915) 857-4545

 

2. DESCRIPTION OF PROJECT

 

International Garment Processors (IGP) facilities are located in East El Paso County, outside the city limits and city services. The IGP plant has a total area of approximately 500 acres. 477.5 acres are dedicated to the aeration pond, irrigation holding pond, and land application of the treated waste water.

 

When the site was being selected, water was (and still is) an important resource for the site requirements, as well as for the residents of El Paso. Mr. Viramontes, the owner of IGP, had the foresight and vision to look for a plentiful supply of water. The water supply is the Hueco Bolson aquifer. Although, the Bolson Basin is an abundant source of water, the water quality is brackish in nature (high in mineral content) and is excluded for consideration by the City of El Paso. The IGP process is the closest industrial water process to "zero discharge" you will find in West Texas.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

At the IGP facilities, water is pumped from the Bolson Basin approximately 600 feet from below the surface. The water is then collected in a large stand pipe which provides a stable and continuous pressure for water demand to the plant. The plant's water is divided into three different streams. They are softened, non-potable and potable. The softened water is subdivided into hot and cold loops for laundry production. The non-potable application are toilets, cooling, and certain portions of laundry process. Potable water is piped to drinking fountains, sinks, and laboratories. The potable water is processed by a Reverse Osmosis System and is chlorinated before it is sent into the plant. Wastewater from the softener's regeneration process and the Reverse Osmosis System is evaporated in evaporation ponds. Waste water from domestic use, i.e. toilets. drinking fountains, etc., is processed through the separate specific system and disposed of through the leach field. .

 

The laundry production waste water is segregated, neutralized for pH and oxidation. After the waste water is collected, it is processed by mechanical filters to a level less than 100 microns. The filtration process leaves the water with a slight blue color. The water is then sent to the ponds for biological decomposition and a natural purification process that is accomplished through "safe" bacteriological decomposition. The water is monitored daily with laboratory analysis completed weekly.

 

Laundry waste water enters the primary holding retention pond for oxygenation via mechanical aerators for forty-five (45) days and then passes through the polishing diffusing aerators. In this portion of the pond, suspended solids and organics are settled and oxidized. After the water reaches the shallow end of the pond, it is transferred to the large polishing pond where water quality approaches a clear quality. This pond is in continuous movement and is aerated by a large venturi pump aerator. This aerator aerates and cools the water as the water cascades through the air over the pond. The aerator also keeps the pond in constant movement. The venturi pumps are the same irrigation pumps that drive the central pivot.

 

The water quality of the irrigation pond is ideal for our farm and pistachio orchard. The farm is watered with a center pivot and alfalfa is raised on 62 acres. The remaining 40 plus acres are used to grow oats in the desert of West Texas.

 

4. ENVIRONMENTAL BENEFIT

 

 

Effluent from Production area

Effluent from irrigation Pond

BOD

600 mg/1

Less than 10 mg/l

COD

1200 mg/1

Less than 200 mg/1

TSS

600 mg/1

Less than 25 mg/1

 

 

5. COST SAVINGS/BENEFIT

 

Considering all the factors involved with a completely. segregated water system (independent from municipal wastewater treatment systems) IGP enjoys cost savings in various areas throughout our operation.

 

One example is IGP's cost per thousand gallons of water. This cost is considerably lower than water purchased from El Paso Water Utilities by about one dollar per thousand. This lower cost includes sewer charges and sewer surcharges which are regularly dealt with by other laundries in El Paso.

 

In short, rather than purchasing, utilizing, and disposing of perfectly good drinking water down the sewer, IGP is putting non-potable "brackish" water to conscientious use. This brackish water is used to wash blue jeans, treated, then used to irrigate cash crops like alfalfa that return some monies into system. The cost benefit we enjoy are in one way assisting municipal treatment plants by keeping tax rates, water rates, sewer rates, and operating costs down.

Last but not least, can you allocate a cost value to protecting the environment? Our answer would be no! Therefore IGP's commitment towards protecting our valuable water resources, no matter what the cost, will benefit the City of El Paso, the State of Texas, and the whole United States by saving millions of gallons of precious drinking water per week.

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International Paper

ipaper4.95

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Texarkana

Number of Employees: 1,050

Industry: Paper and Paperboard Manufacturing

Waste Reduced: Paper by-products

Process: Recycling

Contact Person: Ken Howorth, (903) 796-1412

 

2. DESCRIPTION OF PROJECT

 

International Paper - Texarkana Mill began a cooperative with the Cass County Resource Recovery Facility (CCRRF). To be successful in recycling, CCRRF was in need of a consumer for its fuel pellets made from fiber-based waste materials. The mill realized several advantages to becoming a consumer for fiber-based fuel. Much of the paper produced at the mill is coated with polyethylene. The coating makes the paper difficult to recycle by conventional means. A program was launched to send the coated paper to the CCRRF to be used in the production of a fiber-based fuel. The mill would in turn purchase the fiber-based fuel for their production processes.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The most innovative aspect of the project is the cooperative effort between the Texarkana mill and the Cass County Resource Recovery Facility. Poly-coated paper has previously been difficult to recycle. Pelletizing the paper by-product into a useable product provides energy, reduces landfilling of solid waste, and protects air quality.

 

4. ENVIRONMENTAL BENEFIT

 

The project keeps solid waste out of the mill's on-site landfill, approximately 22,000 cubic yards per year. The recycling efforts of the Cass County Resource Recovery Facility reduce solid waste at the regional landfill. Air quality increases by providing the mill with a cleaner burning, renewable fuel source. Burning fiber-based fuels when compared with fossil fuels results in air emission reductions of 21 percent sulfur dioxide, 10-20 percent carbon monoxide, and 67.7 percent nitrogen oxide.

 

5. COST SAVINGS/BENEFITS

 

The cost to the mill is essentially zero, CCRRF supplies dumpsters and transportation. The purchase price of pellets is slightly higher when compared to bark, but the mill is expected to break even. The reduction in onsite landfill results in a savings of $220,000 per year.

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Jones Blair Company

jonesb1.94

1. GENERAL INFORMATION

 

Location: Dallas

Number of Employees: 250

Industry: Coatings

Waste Reduced: Wastewater

Process: Water Reuse, Painting

Contact Person: Carlos E. Dorris, (214) 353-1660

 

2. DESCRIPTION OF PROJECT

 

Jones Blair has achieved zero discharge of wastewater from its facility of 12 plus acres with a Paint Plant, Resin Plant and Powder Coating unit on site. Jones Blair employees are the key to its success in pollution prevention. They are involved in every step the company takes. The company meets monthly with them in Resin SPC, Paint SPC, Powder Coating SPC, Waste Reduction and Rework committee meetings.

 

This success has not been without lots of dead ends, but the employees never lose sight of the company's goal (zero discharge). The water treatment plant is designed to treat 5,000 gallons of waste water. Jones Blair reuses and recycles water first; the water treatment plant is the last step. Storm-water is also treated and reused. The presense of the Resin Plant makes any rain water hazardous and must be pretreated before discharge. Instead of discharge the company treat and reuses/recycles the water. Its new hot water latex tank washer has eliminated spoiled batches caused by bacterial contamination.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

 

No process water or storm water is discharged. All water is recycled and reused.

 

  1. COST SAVINGS/BENEFIT

 

Cost savings include $17,000/yr. in regulatory fees, $17,500/yr. from reduced water use in cooling towers, and $12,000/yr. in disposal costs.

 

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Kelly Air Force Base: Chromates

kelly1.94

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: San Antonio

Number of employees: 13,000

Industry: Metal Fabrication

Waste Reduced: Wastewater, Chromate

Process: Chemical Substitution, Aluminum Anodizing

Contact person: Greg Vallery, (210) 925-3100

 

2. DESCRIPTION OF PROJECT

 

Kelly AFB Aircraft Directorate has an anodize process located at the bonding shop anodize line in Bldg. 375. This process uses a chromated deoxidizer. Chromium can exist as either trivalent or hexavalent chromium. Hexavalent chromium is a carcinogen and causes a wide range of systemic effects on humans. Chromium causes adverse acute and chronic effects in aquatic organisms. EPA lists chromium as a hazardous waste due to its toxicity characteristic (EPA Waste Code D007) at a concentration of 5 ppm. This project is designed to reduce the use of Chromium which is an EPA 17 ITP chemical by chemical substitution.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The chromated deoxidizer was replaced with a Boeing patented Phosphoric Acid Deoxidizer (PAD).

 

4. ENVIRONMENTAL BENEFIT

 

This project eliminated approximately 1,000 pounds/year of sodium dichromate, an EPA 17 ITP chemical, reducing the chromium load on the base Industrial Waste Treatment Plant.

 

  1. COST SAVINGS/BENEFIT

 

Cost savings on materials alone is approximately $1,100/yr.

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Kelly Air Force Base

kelly3.94

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: San Antonio

Number of employees: 13,000

Industry: Metal Fabrification

Waste Reduced: Wastewater, Cyanide Stripper

Process: Equipment Modification, Metal Stripping

Contact person: Dave Leeson, (210) 925-3100

 

2. DESCRIPTION OF PROJECT

 

Large amounts of cyanide solutions were used in metal refinishing operations. These included solutions to strip plate metals and other surface coatings form aircraft parts (strippers), to clean and remove smut from parts in preparation for electroplating (cleaners), and to electroplate metals onto parts (plating solutions).

 

Cyanide strippers have been used commercially to strip a large variety of plate metals and other surface coatings from a number of metallic and nonmetallic substrates. Cleaning solutions use cyanide for the removal of rust, scale, and smut. They become saturated with metals and other contaminants until no longer effective and require replacements. The project involved a material change (chemical substitution).

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The replacement of all cyanide metal strippers with non-cyanide metal strippers has been implemented for nickel and silver strippers (Metalx B-9 nickel stripper and Rosstrip 999-sp electrolytic silver stripper and Clepo 204 metal stripper).

 

4. ENVIRONMENTAL BENEFIT

 

This material change reduced the use of Cyanide which is an EPA 17 ITP chemical. Cyanide rinse waters also pose a serious health threat to workers and the environment. By eliminating cyanide strippers, Kelly AFB reduced the amount and toxicity level of its hazardous waste stream.

 

  1. COST SAVINGS/BENEFIT

 

This project has an economic savings of approximately $100,000/yr in disposal costs alone.

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Lone Star Radiator Company, Inc.

lonestar.95

1. GENERAL INFORMATION 1995 Governor's Award

 

Location: San Antonio

Number of Employees: 12

Industry: Radiator Repair

Waste Reduced: Wastewater, Metals

Process: Water Reuse

Contact Person: David Bippert (210) 732-7558

 

2. DESCRIPTION OF PROJECT

 

Water from from our operations contains heavy metals that make the water hazardous. This can no longer be discharged to the city's sanitary sewer and there are few waste haulers able to handle the waste (and it is expensive to have them haul it off).

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

Lone Star located a system produced by E/CAR Environmental that utilizes chemical treatment to remove oil products and heavy metals. The heavy metals and other solids drop out of the solution as a sludge and the water can be reused for general cleaning in the shop. The sludge is dried and shipped to a certified recycler (Concorde-Houston) who reclaims the metals. Likewise, the petroleum products are sent to a recycler.

 

4. ENVIRONMENTAL BENEFIT

 

This closed loop process eliminated the disposal of hazardous wastewater and reduced water needs by 36,000 gallons a month. Lone Star was the first radiator shop in San Antonio to install this closed loop system.

 

5. COST SAVINGS/BENEFITS

 

The entire system cost about $40,000. To dispose of 36,000 gallons of hazardous waste a month would have cost well over $100,000 each month.

 

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Murdock Engineering Company: Hexavalent Chromium

murdock 1.92

1. GENERAL INFORMATION

 

Location: Irving, Dallas County

Number of Employees: 212

Industry: Metal Fabrication

Waste Reduced: Wastewater, Hexavalent Chromium

Process: Recovery, Electroplating

 

2. DESCRIPTION OF PROJECT

 

A Hexavalent Chromium Regeneration Unit (HCRU) has been developed and installed on Murdock's sulfuric acid-sodium bichromate deoxidizer process tank which oxidizes trivalent chromium to the hexavalent state and removes extraneous cationic metal contaminants without interfering with production. The HCRU is applicable for eliminating waste streams commonly generated from solutions containing hexavalent chromium in etchants, plating solutions, deoxidizers, anodizing solutions, chem film, and similar processes.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The HCRU utilizes electrodialysis technology whereby an anode cell is fitted on either side with a cationic selective membrane that has an anode suspended inside. The cell is suspended into a tank of catholite solution with a cathode suspended on either side of the anode cell adjacent to the membrane window. The process solution (anolite) is pumped to the bottom of the cell and gravity flows from the top of the cell back to the process tank. As the anolite rises through the cell, a current flow between the electrode plates oxidizes trivalent chromium to the hexavalent state and attracts cationic metal contaminants through the membrane into the catholite solution; thus, the process solution is maintained at a comparable fresh bath state.

 

The HCRU can be operated intermittently or continuously as needed to maintain solution integrity. It is free standing and is located so as not to interfere with production. All parts are commercially available for ease of servicing.

 

4. ENVIRONMENTAL BENEFIT

 

The environmental impact from use of the HCRU is very significant in that the process solution is never depleted due to normal process contaminants.

 

Specific benefits are:

* Oxidizes trivalent chromium to the hexavalent state

* Extracts dissolved metal contaminants from the process solution

* Maintains consistency of process solution resulting in uniform processing

* Lowers solution viscosity which reduces rinsewater dragout contamination

* Eliminates downtime due to spent solution change out

* Eliminates fresh bath make-up chemical cost

* Eliminates the ever increasing cost of hazardous waste disposal and associated

liabilities

 

  1. COST SAVINGS/BENEFIT

 

Cost savings associated with use of the HCRU will vary depending on chemical

composition, type and quantity of materials processed, and the volume of process solution.

 

Typical Performance on Deoxidizer Solution (1988 Data)

* Solution: Sulfuric Acid 37.6-39.3 oz/gal Sodium Bichromate 4.1-5.0 oz/gal

* Temperature: 155-160'F

* Tank Volume: 1870

*Trivalent Chromium: 1.9 percent by weight maximum

Cr+6 Cr+3 A1+3 REMARKS

HCRU Start Up 4 .22 Limit 1.1623 .748 Cr+6 Near low

 

HCRU Shut Down 4.963 .7519 .653 Cr+6 Near

high limit

Change (percent) +17.6 -35.3 -12.7 Run Time: 74 Hrs.

 

Cost: Approximately $3.79

 

Cost prior to HCRU installation: (Low production period)

 

Chemical Disposal: Approximately $ 9,000

Replacement Chemicals: 2,800

TOTAL $11,800 x an average of twice a year

Production Downtime: Two days

Hazardous Waste Liability: Forever

 

The HCRU was developed for Murdock's own need and use. After the system was tested and proven in a production environment, Murdock patented the device with the intention of producing HCRUs as a commercial product line.

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Texas Eastman: Organic Waste

txeast15.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Longview, Harrison County

Number of Employees: 2,700

Industry: Chemicals, Organic

Waste Reduced: Wastewater

Process: Drift Reduction, Cooling Towers

Contact Person: Glenn Phillips, (903) 237-5346

 

2. DESCRIPTION OF PROJECT

 

The ethylene glycol department has two cooling towers that cool and recirculate process water streams that contain about 8% ethylene glycol. As the air is pulled through the falling water a small percentage of water and ethylene glycol is released to the atmosphere. Besides being a loss of product, the emissions of ethylene glycol has to be reported.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The department formed a team to look at ways of reducing emissions. They found that new technology existed to reduce drift from cooling towers. The new design allows the drift to impinge on baffles and the droplets that are formed then drop back into the tower instead of going out over the tower. The total cost of the project was $55,000.

 

4. ENVIRONMENTAL BENEFIT

 

Ethylene glycol emissions were reduced by 72,000 pound per year with the new drift eliminators.

 

5. COST SAVINGS/BENEFIT

 

Sales of recovered ethylene glycol is about $18,000 a year.

 

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Texas Eastman: Waste Oil Burning

txeast6.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Longview, Harrison County

Number of Employees: Approximately 2,700

Industry: Chemicals, Organic

Waste Reduced: Wastewater

Process: Water Recovery, Waste Oil Burning

Contact Person: Glenn Phillips, (903) 237-5346

 

2. DESCRIPTION OF PROJECT

 

Texas Eastman cracking plants mix large amounts of steam with feedstock before cracking it into ethylene and propylene. After the steam leaves the reactors it is condensed. Because the condensed water contained various oily materials it had to be treated. Utilities also had to purify the water coming into the facility before it could be used in the process. Both fresh water purification and wastewater treatment are expensive.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

A new process water recovery unit was constructed. The unit removes oily contaminant from the condensed water by a DOXTM coalescing unit supplied by Nalco, Inc.. The water is turned back into steam for continuous reuse in the cracking process. The oils from the recovery process are reused as a heat transfer oil and eventually sold as a product.

 

4. ENVIRONMENTAL BENEFIT

 

Wastewater treatment was no longer needed for 105 million gallons of wastewater per year. Also, since the oily contaminants are recovered, there is a reduction in VOC emissions by about 60,000 pounds a year.

 

  1. COST SAVINGS/BENEFIT

 

Costs savings come from reduced treatment of fresh and waste water and from reduced fuel needs for the cracking unit.

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Texas Instruments

62.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Sherman, Grayson County

Number of Employees:

Industry: Electronics

Waste Reduced: Wastewater Metals

Process: Wastewater Treatment, Reducing Chelating

Contact Person: Norm Carlson, (903) 868-5722

 

2. DESCRIPTION OF PROJECT

 

The project encompassed development and incorporation of a waste treatment process for alkaline soak cleaners used in our aluminum chemical finishing processes.

 

The chelating agents in our cleaners were tying up the heavy metals (in particular chromium, the major contaminant) in our waste chemical streams. This prevented complete precipitation of the chromium for proper filtration removal in our waste treatment facility.

 

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

The old method of disposal was to have the cleaning solutions either drummed up or placed in a tank truck for off-site disposal. This was not desirable due to trucking/disposal costs and potential liabilities.

 

Another method of disposing of the solution was suggested by the manufacturer of the cleaning solution. This method involved breaking the chelating effect, thereby rendering the solution treatable through our existing waste treatment facility. The chelating effect was broken by adding calcium oxide (lime), mixing the treated solution for one hour, and finally adding the mixed solution to the waste treatment pH adjust tank at a controlled rate for treatment. While the calcium oxide (lime) treatment process was an alternative, there was the cost of additional process equipment (mixing tank, mixer, metering pump, etc.) and time involved.

 

Another alternative investigated was reducing the rate at which the cleaner was metered into the waste treatment process. While this did reduce the level of chromium in the effluent, the levels exhibited with practical cleaner flow rates still did not provide chrome levels below 1 ppm (total chrome), as desired.

 

One final study was initiated. This involved the possible use of nucleation agents to improve the precipitation process. Some of the possible nucleating agents were coprecipitated metals such as copper, nickel, zinc, iron, calcium, aluminum or cationic polymers. Looking for a

 

naturally occurring source of one of the above metals, the concept for possible use of aluminum, which builds up in our alkaline etch solution was researched.

 

A 50/50 mix of the waste soak cleaners and alkaline etch solutions, when added at low percentages by volume of reduced chrome solution, provided satisfactory chrome levels in the waste treatment process effluent. This was, in part, due to the dissolved aluminum in the alkaline etch acting as a nucleating agent for more effective precipitation of heavy metals, while reducing the effects of the chelating agents in the cleaners.

 

4. ENVIRONMENTAL BENEFIT

 

This use of waste alkaline etch solutions provided an innovative means for improved inhouse treatment of alkaline soak cleaners, thereby eliminating the costs and liabilities of having to transport these waste solutions (some 1600 gallons/year) off-site for disposal.

 

5. COST SAVINGS/BENEFIT

 

This process saved some $2300/year in trucking/disposal costs per tank, while being a process which was accomplished without the cost of additional equipment and processing time.

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Witco, Inc.: Three Projects

Witco, Inc.: Project 1

witco1.94

1. GENERAL INFORMATION

 

Location: Marshall

Number of Employees: 60

Industry: Chemicals, Organic

Waste Reduced: Wastewater

Process: Equipment Modifications, Cooling Towers

Contact Person: Bill Childers, (903) 938-5141

 

2. DESCRIPTION OF PROJECT

 

Witco installed two automatic chemical controls for blowdown on cooling towers. The system maintains a set conductivity for the water in the tower. It saves water (and chemical additives) over periodically adding fresh water on a timed bases.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

 

The system has reduced the quantity of blowdown water and chemical additive use by 50%. Approximately 720,000 gallons of water is saved per year.

 

  1. COST SAVINGS/BENEFIT

 

The two units purchased cost $2,000 each for a total of $4,000. At $0.001/gallon, water use savings amounted to $720 annually. More significantly, chemical additives were reduced saving $3,300 annually. Wastewater disposal costs for clean cooling tower water runs about $0.025/gallon, for a savings of $18,000.

 

Witco, Inc. Project 2

witco2.94

1. GENERAL INFORMATION

 

Location: Marshall

Number of Employees: 60

Industry: Chemicals, Organic

Waste Reduced: Wastewater

Process: Equipment Modifications, Tank Cleaning

Contact Person: Bill Childers, (903)938-5141

 

2. DESCRIPTION OF PROJECT

 

Process equipment is frequently washed down when switching products. Using the old procedure, the equipment was filled with water, agitated and dropped to waste. Special spray nozzles (designed for cleaning tank cars) were installed to reduce the amount of water needed to clean this equipment.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

 

The use of the spray heads resulted in reducing water use and disposal of 100,000 gallons a year.

 

  1. COST SAVINGS/BENEFIT

 

A total of 4 spray heads were purchased at $40 each, for a total cost of $160. Water costs are $0.001/gallon for an annual savings of $100. More significantly, deep well injection of wastewater costs about $0.05/gallon, for an annual savings of $5,000.

Witco, Inc. Project 3

witco I .95

1. GENERAL INFORMATION

 

Location: Marshall

Number of Employees: 60

Industry: Organic Peroxides

Waste Reduced: Process Cooling Water

Process: Interupt Spray

Contact Person: Bill Childers, (903) 938-5141

 

2. DESCRIPTION OF PROJECT

 

Witco produces organic peroxides and peroxyesters for the plastics and fiberglass industry. The product is washed with a KOH solution to remove impurities and separated in a centrifuge. A water mist system is used in the centrifuge to cool the system to prevent product decomposition. The separated water is hazardous for pH and organic content and is sent to deep well injection for disposal. By measuring cooling water use, temperature and product quality it was determined that the continuous water mist could be replaced by an interrupt system reducing water use significantly.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

 

Reducing water use in the cooling system reduced the total quantity of hazardous waste water that was being generated by over 1 million gallons a year.

 

5. COST SAVINGS/BENEFIT

 

The interrupt system cost $5,000 to install, but saves Witco $26,000 a year in water use and disposal costs.

 

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