Wastewater Case Studies
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Case Studies: Wastewater

Witco
Sandoz Crop Protection
Texas Eastman Wastewater

Texas Eastman Chloroform

Texas Instruments Wastewater

Transport Service Company

Union Carbide - Seadrift Plant

Valero Refining

Alumax Mill Products

Amoco Oil Company

Anheuser-Busch

Bell Helicopter Textron Inc

CDC Coatings/Dickson Weatherproof Nail Co.

CMI, Texas, Inc.

E. I. du Pont de Nemours & Company

E. I. du Pont de Nemours & Company- VOC

E. I. du Pont de Nemours & Company-Oil

E.1. du Pont de Nemours & Company-Ehylene

GCA-Washburn Tunnel Wastewater

GCA-Washburn Tunnel-Energy Efficiency

Go/Dan Industries

Hoechst Celanese

Hoechst Celanese- Leachate

Huntsman Corporation Port Neches

Huntsman

Motorola

Motorola-Hydrofluoric Acid
Oxy Petrochemicals, Inc.
Oxy Petrochemicals, Inc.
-Copper
Phillips Petroleum Company

Phillips Petroleum Company-Artificial Marsh

Rhone Poulenc

Rhone Poulenc-Copper


 


Witco,Inc.

witC03.94

1. GENERAL INFORMATION

 

Location: Marshall, Texas

Number of Employees: 60

Industry: Chemicals, Organic

Waste Reduced: Wastewater

Process: Water Reuse

Contact Person: Bill Childers. (903) 938-5141

2. DESCRIPTION OF PROJECT

Witco collects "clean" wastewater for reuse in non-critical areas. Boiler, cooling tower blowdown and other utility area wastewater is collected and reused for services such as floor sprays and wash water. This eliminates the use of fresh water in these application and, as a result, reduces the quantity of fresh water use.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

By reusing brown water for non-critical use Witco reduced water usage by 2,000,000 gallons a year. Some rain water was also collected in the system, so the total reduction in water disposal was 2,824,000 gallons.

5. COST SAVINGS/BENEFIT

 

Witco used an existing 5,000 gallon tank to store brown water. Pump, pipe, controls and other installation costs amounted to $20,000. Freshwater cost $0.001/gallon saving $2,000 annually. Disposal cost for "clean" wastewater runs about $0.025/gallon for an annual saving of $70,600.

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Sandoz Crop Protection

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1. GENERAL INFORMATION

 

Location: Beaumont, Texas

Employees: 300+

Industry: Chemicals, Agricultural

Waste Reduced: Process Chemicals, Chlorinated Organics

Process: Recycling

Contact: Rob Swinney, (409) 722-8061

2. DESCRIPTION OF PROJECT

Our facility manufactures four agricultural herbicides and one insecticide product. The manufacturing processes generate both hazardous and non-hazardous waste chlorinated compounds which at one time were all being transported off site for incineration and landfill. In 1990 an onsite facility was engineered and constructed to thermally destroy the chlorinated waste compounds while at the same time recovering the chlorine, hydrogen, and oxygen to produce 14% aqueous hydrochloric acid for use as a raw material in one of the manufacturing processes.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

Rather than disposing of the waste or just incinerating the compounds, a useful product is generated in the process which can be used on site.

4. ENVIRONMENTAL BENEFIT

From 1990 through 1993 the facility generated over 12,700,000 pounds of waste chlorinated compounds. Over 16,000 tons of hydrochloric acid was produced from that waste and used as a raw material in the manufacturing process.

 

5. COST SAVINGS/BENEFIT

 

The disposal cost for these compounds would have been $4,000,000 and the additional purchases of HC I would have amounted to $2,000,000. The initial cost of the unit was $6.5 million and it has an operating budget of $1.3 million per year.

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Texas Eastman Wastewater

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

Location: Longview, Harrison County

Number of Employees: 2,700

Industry: Chemicals, Organic

Waste Reduced: Wastewater

Process: Recycling, Wastewater Treatment

Contact Person: Neil Quinn, (903) 237-5474

 

2. DESCRIPTION OF PROJECT

Wastewater from several thermal cracking plants is pretreated to remove aromatic oil prior to its discharge to the company's wastewater treatment system. The characteristically hazardous oil was previously burned for fuel value in the company's boilers. The oil is now being recycled to another thermal processing plant as a substitute for a commercial chemical product. This project has reduced the amount of hazardous waste being burned for fuel.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

This project involved process development work in order to determine that the oil could be substitute for a commercial chemical product in another process while still maintaining product quality in the process.

4. ENVIRONMENTAL BENEFIT

Generation of hazardous waste burned for fuel value was reduced by 1.9 million gallons per year.

5. COST SAVINGS/BENEFIT

Savings due to reduced purchased of commercial product less cost of additional natural gas to replace oil for fuel were approximately $ 800,000 per year.

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Texas Eastman Chloroform

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Longview, Harrison County

Number of Employees: 2,700

Industry: Chemicals, Organic

Waste Reduced: VOC Emissions, Chloroform

Process: Air Stripping, Wastewater Treatment

Contact Person: Glenn Phillips, (903) 237-5346

2. DESCRIPTION OF PROJECT

Tests determined that natural gas could strip chloroform from wastewaters and carry it to a hazardous waste incinerator. The wastewater from the acetaldehyde production facility typically contained 10 ppm chloroform. In 1988 the EPA proposed a regulation that limited chloroform in wastewater to 100 ppb before biological treatment. The chloroform in the wastewater was reduced to 25 ppb by using the gas stripper.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

A pilot study confirmed that natural gas could be used to extract chloroform from the waste water.

4. ENVIRONMENTAL BENEFIT

The gas stripper reduced the chloroform in the waste water by 400 fold to 25 ppb. It also reduced other waste such as benzene and dichloromethane by 20 fold.

5. COST SAVINGS/BENEFIT

There are substantial environmental benefits in emission reductions, but no cost savings.

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Texas Instruments Wastewater

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Stafford, Fort Bend County

Number of Employees:

Industry: Electronics

Waste Reduced: Wastewater

Process: Water Recovery, Parts Cleaning

Contact Person: Cherri Paluch, (713) 274-2043

Patrick Williams, (713) 274-3330

2. DESCRIPTION OF PROJECT

In the Source Rebuild Shop, contaminated parts are cleaned with a water-based abrasion system. The water is cycled through a settling tank and the clean water is then recirculated through the process.

The employees from the manufacturing area decided to address a related solid hazardous waste as a part of the Total Quality Culture Effectiveness Team program. During their research, they discovered several areas for waste minimization improvements. The largest improvement was utilizing the Source Rebuild Shop's hazardous waste compactor to its full potential. By re-educating the area workers and improving access to the compactor, the team projects a 80% reduction in volume. The team is also evaluating improved handling procedures.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

A specialized ionic exchange resin bed was evaluated, at first, to remove the contamination from the wastewater before its disposal. While the resin was reasonably effective, it could not meet the low disposal limits under the site's NPDES permit. The recirculation system and settling tank was developed as a better alternative.

4. ENVIRONMENTAL BENEFIT

The water recirculating system has reduced hazardous wastewater generation from the Shop by 2,050 gallons, 97% by volume. The Effectiveness Team projects an 80% reduction in solid hazardous waste volume.

5. COST SAVINGS/BENEFIT

The direct disposal cost savings are $59,940 for the wastewater and $85,500 for the solid waste.

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Transport Service Company

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1. GENERAL INFORMATION

 

Location: Freeport, Brazo County

Number of Employees: 57

Industry: Transportation

Waste Reduced: Wastewater

Process: Wastewater Treatment

Contact Person: Alan W. Dunaway, (713) 474-7621

2. DESCRIPTION OF PROJECT

Bio-treatment of tank cleaning generated waters.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

The application of biological systems for remediation and control of environmental processes has greatly increased in recent years. Employing bio-remediation, pollutants are degraded into products that are part of naturally occurring cycles.

Degradation of hazardous and toxic wastes employing naturally occurring bacterial cultures go hand in hand. Transport Service Company has merged this process into an industrial wastewater treatment system.

Equipment used to facilitate this process includes: air pumps, fine air diffusers, pH control mechanisms, holding tanks and a separator for primary treatment.

4. ENVIRONMENTAL BENEFIT

Benefits include the reduced toxicity of generated wastewaters via naturally occurring organisms.

5. COST SAVINGS/BENEFIT

Financial benefits include reduction of man hours associated with the previous treatment process. Operational cost have been substantially reduced. Most importantly, though, are the reduction in surcharges imposed by the POTW for secondary treatment. These surcharges annually are $20,000.00.

 

Payback on project estimated at 1.5 years.

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Union Carbide - Seadrift Plant

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Port Lavaca, Calhoun County

Number of Employees: 1,150

Industry: Chemicals, Plastic/Resin

Waste Reduced: VOC Emissions

Process: Equipment Modifications

Contact Person: Rick Curtis, (512) 553-2435

2. DESCRIPTION OF PROJECT

Union Carbide's Seadrift Plant has completed an extensive project to improve our wastewater treatment system. Two earthen water treatment lagoons have been replaced with modern fully enclosed, 5.5 acre wastewater treatment reactor. The new system will improve the biodegradation of organics and will essentially eliminate organic off-gas emissions normally associated with treatment systems.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

The replacement lagoon itself is designed and constructed in accordance with federal surface impoundment guidelines. While not mandatory, the system has a 5.5 acre 100 ml floating HDPE cover over the entire area to contain odors that would be generated.

4. ENVIRONMENTAL BENEFIT

This project benefits the environment as a result of the protection which it provides for the earth and groundwater, as well as the air and water. A total reduction of 800 tons/year of hydrogen sulfide and 12.5 tons/year of VOC's to the air has been achieved.

 

5. COST SAVINGS/BENEFIT

In addition to the environmental benefit, the odors from the treatment system are dramatically reduced, which also benefits employees and near-neighbors.

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Valero Refining

valero2.95

1. GENERAL INFORMATION 1995 Governor's Award

 

Location: Corpus Christi

Number of Employees: 485

Industry: Refining/RFG Gasoline

Waste Reduced: Slop Oil Emulsion Solids

Process: Oil/Water/Solid Separation

Contact Person: Allen Schoen, (512) 289-3285

2. DESCRIPTION OF PROJECT

Valero staff began reviewing waste water streams in 1992 to determine if there were advantages to processing waste water prior to entering the waste water treatment (WWT) system. Analysis indicated that the desalters contributed about 237 gpm of water (221 gpm), solids (6266 ppm) and oil (16.4 gpm) mixture to the WWT system. When the desalter waste water is mixed with other refinery waste waters in equalization tanks, the slop oil emulsion solids are dispersed and adhere to more solids suspended in the water. Tank cleaning requires separation of the slop oil emulsion solids, adding significantly to the cost of the process and generation of "K" listed hazardous wastes.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

Lion Resources, a Corpus Christi company, introduced Conoco's Vortoil' Separation Systems to Valero. The system uses a hydrocyclone principle to remove hydrocarbons and solids from the waste water of Valero's Residual Hydro-Desulfurization Desalter. The separated oil (21,330 BPY) is recycled into the refinery. The waste water goes to the WWT system. The separated solids (85,325 BPY) are treated in Valero's Bioslurry Reactor, described in a previous case study.

4. ENVIRONMENTAL BENEFIT

The Vortoil' systems expected to reduce the generation of oily waste water in WWT system; and, the aggregate generation of hazardous waste in the WWT system equalization tanks by about 350 tons per year. The oil removal allows Valero to continue to reduce VOC emissions from the WWT system.

5. COST SAVINGS/BENEFITS

 

The project was determined to have more than a five year return based on measurable factors: however, Valero, considered the project to be "worthwhile" because it could be used to determine the feasibility of using the technology on other waste water streams of the refinery, it reduced the mixing with other refinery waste water and redundant separation and the aromatics removal allows Valero to reduce NESHAP emissions in its WWT system.

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Alumax Mill Products

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1. GENERAL INFORMATION

Location: Texarkana, Bowie County

Number of Employees: 400

Industry: Aluminum Products

Waste Reduced: Wastewater, Chromium

Process: Electroplating

2. DESCRIPTION OF PROJECT

The source reduction system is for chrome conversion 6 to chrome 3 by chemical precipitation using sodium metabisulfite at a 2.0 pH. Magnesium hydroxide is added for pH adjustment along with sodium hydroxide. Polymers are added to the metal hydroxide solution to facilitate fall out and filtered through a 6 cubic foot press. This filter cake is then fed to a JWI sludge dryer at about 70% water content and dried to approximately 30% water content. This procedure has about a 4:1 ratio of reduction to the sludge being produced. As a waste being recycled and recovered the 30% water must remain to be processed. If Alumax did not have this limitation we could reduce the outgoing waste even further.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

This project has only been facilitated in the last 60 days. The operation is constantly being refined by using statistical process control techniques. These developments can produce management control from the production line all the way to the recycling of the sludge.

4. ENVIRONMENTAL BENEFIT

This type of project allows for the recycling and reusing of wastes. Since the creation of another waste stream is therefore prevented, the problems associated with having to landfill are avoided.

5. COST SAVINGS/BENEFIT

Cost savings have been justified by reducing the sludge volume. The continuing adjustments to fine tune the process will eventually impact chemical usage and sludge production. In turn, costs will be lowered. The payback period of the project is forecast at 3 years.

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Amoco Oil Company

amoco 1.92

1. GENERAL INFORMATION

Location: Texas City, Galveston County

Number of Employees: 2,200

Industry: Oil Refinery

Waste Reduced: API Separator Sludge

Process: Recycling

Contact Person: S. A. Medley-Perry, (409) 945-1151

2. DESCRIPTION OF PROJECT

The Amoco Oil Company refinery in Texas City is utilizing a combination of pressure filtration and coking to reduce the quantity of listed hazardous waste (K048, K051) disposed by 90-95%. The hazardous wastes (DAF float and API separator sludge) are first pressure filtered to recover oil and dewater the wastes. The resulting filter cake is then sent to the refinery coker and converted into fuel-grade coke and oil, in a proprietary Amoco process.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

Although many refineries are using their cokers to minimize waste disposal, the Amoco process is unique in that it involves re-slurrying the filer cake to a pumpable material, The filter cake slurry is then injected into the coker during the coking cycle to recover additional valuable oil and insure complete conversion of hydrocarbons to coke.

4. ENVIRONMENTAL BENEFIT

This project epitomizes resource conservation and recovery. A material that would otherwise be incinerated and lost forever is being recovered and converted into oil and fuel.

 

5. COST SAVINGS/BENEFIT

 

Economic savings have been dramatic, with costs estimated at half the current price for incineration and disposal. Capital costs of the project were recovered in less than a year.

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Anheuser-Busch

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1. GENERAL INFORMATION

 

Location: Houston, Harris County

Industry: Malt Beverage

Waste Reduced: High BOD Water

Process: Wastewater Treatment

Contact Person: Anne Horbaniuk, (713) 678-3713

2. DESCRIPTION OF PROJECT

Prior to installing an eight (8) stage residuals evaporator, Anheuser-Busch collected several process effluent streams, centrifuged these streams to remove solids, and then sewered the centrifuge effluent. This sewered centrifuge effluent was high in BOD and represented 40% of the plant's total loading.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

To eliminate this portion of our BOD stream, Anheuser-Busch purchased and installed an eight (8) stage residuals evaporator. The centrifuge effluent is now pumped to an evaporator feed tank, rather than to the sewer. From the feed tank, it is metered into the multiple stage evaporator. Moisture is removed as a condensate stream leaving behind a concentrated thick syrup with approximately a 50% total solids makeup. This syrup is then sold to a liquid animal feed producer.

This evaporator application is present throughout the brewing and distilling industry. Here at Houston, the plant has been able to bring the evaporator up and operate per design spec within six months.

4. ENVIRONMENTAL BENEFIT

By installing the residuals evaporator, Anheuser-Busch reduced the amount of BOD loadings per day to the sanitary sewer by about 22-23,000 pounds (8 million pounds for 1993). Thus, impacting favorably the local sewer treatment plant.

5. COST SAVINGS/BENEFIT

The evaporator should yield an annual sewer savings of approximately $1,500,000. It will increase our fuel, water, and electric costs. The plant will earn some revenues from the sale of the brewers condensed solids. Total project payback is five (5) years.

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Bell Helicopter Textron Inc.

bellhe1 1.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Fort Worth, Tarrant County

Number of Employees: 4,000

Industry: Metal Parts Fabrication

Waste Reduced: Sludge

Process: Wastewater Treatment, Neutralization

Contact person: Debra L. Rodriguez, (817) 280-8729

2. DESCRIPTION OF PROJECT

Bell Helicopter Textron Inc. has replaced lime with magnesium hydroxide as a neutralization agent at our wastewater treatment plants. Bell is saving money, providing a safer working environment for our employees and reducing our annual hazardous waste sludge.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

Metal finishing processes at Bell generate a variety of acidic waste streams containing dissolved toxic metals. Before the wastes may be discharged to a sewer or receiving stream, the pH of the solution must be adjusted to an acceptable level and the metals removed. These acidic waste streams are commonly neutralized by adding caustic soda or lime, both are strong bases. Magnesium hydroxide, a fairly weak base, has been used for years as a neutralizing agent for acids. It is the major ingredient in such medicines as "Milk of Magnesia", but has rarely been used in wastewater treatment.

Magnesium hydroxide can be easily purchased as an aqueous white slurry with a density between 12.3 and 12.5 pounds per gallon. The slurry is 55-60% magnesium hydroxide by weight and is similar to latex paint in consistency and appearance.

A convenient way of comparing magnesium hydroxide to lime or caustic soda is to look at neutralization strength on a weight basis. Magnesium hydroxide has 27% more hydroxyl ions than lime and 37% more than caustic soda. Thus, it takes less magnesium hydroxide to neutralize a given amount of acid or to remove a given amount of metals.

4. ENVIRONMENTAL BENEFIT

Slower reaction time of magnesium hydroxide produces denser solid particles of metal hydroxides than with lime or caustic soda. Magnesium hydroxide is a weak base and forms solutions that are buffered or resistant to changes in pH. Therefore, acids neutralized with magnesium hydroxide form solutions that are buffered within a pH range of 9.0 to 9.4. This means that adding too much magnesium hydroxide will not push the pH above the limits allowed for discharge to most sanitary sewers.

The by-products produced when magnesium hydroxide neutralizes sulfuric acid is magnesium sulfate (epsom salts) and is soluble and may be discharged safely to the sanitary sewer.

Bell Helicopter's operators found magnesium hydroxide was much easier to use and more predictable than lime. Besides saving time while neutralizing tanks, the lessened volume of hazardous waste greatly reduced the time required to condition and dry the sludge. The only disadvantage noted was a slight increase in the amount of flocculating polymer required.

5. COST SAVINGS/BENEFIT

Bell Helicopter has realized a real reduction in the volume of greater than 50% or 500 tons of hazardous waste sludge per year. This translates to a net annual savings of over $220,000 and greatly reduces our liability due to less sludge being disposed of per year.

Bell Helicopter has also gained benefits from improved safety conditions, reduced maintenance requirements and an easing of the work load for the wastewater treatment operators. In addition, a nonhazardous material has been substituted for a very hazardous material. Magnesium hydroxide is safer for employees and the environment. Bell Helicopter was able to convert over to magnesium hydroxide with little capital equipment investment. Our greatest payback is in the fact that Bell's largest and costliest hazardous waste stream was greatly reduced, thereby reducing our cost and liability.

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CDC Coatings/Dickson Weatherproof Nail Co.

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1. GENERAL INFORMATION

 

Location: Houston, Harris County

Number of Employees: 90

Industry: Metal Parts Fabrication

Waste Reduced: Wastewater

Process: Recovery

Contact Person: Gary Edwards, (713) 452-6429 ext. 205

2. DESCRIPTION OF PROJECT

CDC Coatings/Dickson Weatherproof Nail Co. manufactures specialty nails and various metal fasteners. A proprietary galvanizing process or special paint coatings are added to their products to provide corrosion protection. These special paints and galvanizing materials used in their process end up in the wastewater as a result of cleaning operations. These materials are removed by their wastewater treatment system prior to discharge.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

The wastewater treatment system experienced difficulty with the settling process during peak production loads. When the system had problems during peak loads, it was necessary to backwash the filters more frequently, which requires additional water to be treated. In an effort to conserve the amount of water being treated, a wastewater recirculation system was installed on a large receiver to improve the wastewater treatment operation.

4. ENVIRONMENTAL BENEFIT

In the past it was difficult to stay under the permit limits for daily maximum flow for the treatment system. The added recirculation system improved the efficiency and reduced the flow through the system to the point where it is no longer difficult to stay in compliance. As a result of improved operation, the daily water usage has been reduced 60 % .

5. COST SAVINGS/BENEFIT

The wastewater recirculation system cost less than $10,000 to install and saved over $156,000 in treatment cost the first year. The payback period was less than 17 days.

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CMI, Texas, Inc.

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1. GENERAL INFORMATION

 

Location: Nuevo Laredo, Mexico

Number of Employees: 800

Industry: Engine Manifolds

Waste Reduced: Wastewater

Process: Ultrafiltration

2. DESCRIPTION OF PROJECT

CMI produces oily waste water from its cutting and cleaning operations. The wastewater was sent to Texas for deep well injection. To eliminate this costly procedure, CMI installed an ultrafiltration unit to separate the oil and water. After separation, the water can be discharged and meets regulatory limits for grease and oil. The oil is sent for energy recovery. CMI is in the process of purchasing an additional reverse osmosis unit that will produce water clean enough to reuse for cleaning.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

CMI was disposing of approximately 3,000 gallons of oily wastewater per day into deep well injection prior to the installation of the ultrafiltration unit.

5. COST SAVINGS

 

CMI is saving over $3,000 a day from reduced disposal costs. The payback period on the ultrafiltration unit was 4 months. With other improvements to reduce generation of oily wastewater now on-line, CMI is still saving over $62,000 a month.

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E. I. du Pont de Nemours & Company

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: La Porte, Harris County

Number of Employees: 1,070

Industry: Insecticide

Waste Reduced: VOC Emissions, Methylene Chloride

Process: Stripping

Contact: R. K. Barger, (713) 470-3027

2. DESCRIPTION OF PROJECT

 

A new wastewater stripping facility was started up in September 1991 at the du Pont La Porte site. This stripper system collects process wastewater from an insecticide manufacturing process in tanks rather than in a pond and removes the volatile organic compounds to ppm levels.

In this facility, all the wastewater streams containing volatile organics are collected in two large feed tanks and steam stripped to remove the volatile organics. The stripped organics are burned in an existing scrubbed incinerator and the volatile-free wastewater is treated in the plant's biotreatment facilities.

With this system, the amount of volatile organics being discharged to the air from the wastewater handling facilities is greatly reduced. The compound of special importance is methylene chloride, a potential carcinogen.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

Since starting up this unit our TRI reported air emissions of methylene chloride from the site has been reduced from over 475,000 pound to less than 47,000 pounds.

 

5. COST SAVINGS/BENEFIT

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E. I. du Pont de Nemours & Company- VOC

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: La Porte

Number of Employees: 1,100

Industry: Agricultural Chemicals

Waste Reduced: VOC Emissions

Process: Wastewater Treatment, Stripping

Contact Person: Linda Stegeman, (713) 470-3753

2. DESCRIPTION OF PROJECT

Stripping, which effectively removes VOC's from wastewater is being used to remove organics (mostly dichloromethane) from a 30-50 gpm wastewater stream. The stripped organics are treated in our RCRA permitted incinerator and the remaining wastewater is treated in our NPDES permitted biotreatment system after testing for organic content. The facility consists of two pretreatment storage tanks, a stean stripper and two post treatment storage tanks.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

Since starting up this unit our TRI reported air emissions of dichloromethane from the site have been reduced from over 475,000 pounds to less than 84,000 pounds.

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E. I. du Pont de Nemours & Company-Oil

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1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

Location: Orange, Orange County

Number of Employees: 2,000

Industry: Ethylene Production

Waste Reduced: Oil

Process: API Separator

Contact Person: Bich Tran, (409) 886-9227

 

2. DESCRIPTION OF PROJECT

In the ethylene plant, there are many oily water waste sources connected to a concrete "API oil/water separator". These sources include heavy by-products removed from the cracked gas quench tower, blowdowns from the amine and caustic columns and miscellaneous equipment, drainage from curbed areas and water decanted from aromatic distillate storage tanks. In the API separator, most of the oil overflows into a chamber and is recovered as heavy aromatic distillate product. The water, along with soluble organics, solids and some oil, underflows to a second chamber. Prior to 1988, this water was pumped to a settling basin where the water and soluble organics underflowed to a biopond. Floating oil and solids were removed for costly off site waste disposal. Nuisance odors were experienced at the basin, and also at the atmospheric vented API separator because of evaporation of volatile organics (including benzene).

 

To reduce waste disposal cost, improved recovery of oil and solids from the oily water stream was needed prior to sending the stream to the basin. To accomplish this, a $1 MM capital project was approved for installation of the following in mid 1988:

* Facilities to combine blowdowns of the amine and caustic system and allow

neutralization of this stream prior to discharge to the API separator. C02 is used to

reduce the pH of the caustic rich stream with the help of a pH control loop. This

improved oil separation in the API separator and provided adequate pH control of the

water stream exit the separator. Sulfuric acid was considered as an alternate

neutralizing agent but was ruled out because sulfates degrade to hydrogen sulfide in

the biopond.

* A dissolved gas flotation (DGF) unit to improve oil separation of the wastewater

exiting the API separator. The DGF unit uses nitrogen for oil and solids removal.

This unit consists of a flocculator, flotation cells with corrugated plates pack, and

high pressure nitrogen saturation system. Water from the API separator is first

routed to the flocculator which is designed for 45 seconds retention time under mild

turbulent conditions. In this section, oil and solids particles flocculate and grow

under gentle agitation. The water then enters a mixing loop where high pressure

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nitrogen saturated water is injected. Because of lower pressure in the mixing loop, the nitrogen is released to form small bubbles. The water stream then enter the flotation cell where nitrogen bubbles float to the surface carrying the floc particles of oil and solids with it. Diagonal corrugated plates provide surface area to improve nitrogen/floc contact. Floating oil and solids are skimmed off from the top of the water. Clean water exits the bottom of the DGF cell and is pumped to the settling basin.

 

In addition, to reduce atmospheric venting of benzene and personnel exposure to it, a new vent system was installed on the API separator at the cost of $70M. This system utilizes a steam ejector to evacuate vapor in the separator thus creating a slight negative pressure in it and prevent benzene leaks to atmosphere. Discharge of the steam ejector is routed to a gas fired steam superheater where the vapor is burned off. To prevent flashback into the separator, the ejector steam rate was designed to provide a minimum velocity three times higher than the flame propagation rate, along with installation of flame arrestor and associated controls.

 

4. ENVIRONMENTAL BENEFIT

 

Operation of the DGF allows reduction of over 2MM lb/yr of oily water waste that would otherwise have to be disposed of off-site. Furthermore, it prepares the waste water stream for further recovery of benzene utilizing the steam stripping process. The new vent system on the API separator reduced approximately 8 M lb/yr of organic vapor, including 4M lb/yr benzene, vented to atmosphere.

5. COST SAVINGS/BENEFIT

After start up of the DGF project, waste disposal cost associated with the oily water settling basin dropped significantly. Although this $1 MM project was justified as environmental necessity project, gross savings on disposal cost was realized at $1.1MM per year, much higher than expected.

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E.1. du Pont de Nemours & Company-Ehylene

dupont3.92

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Orange, Orange County

Number of Employees: 2,000

Industry: Ethylene Production

Waste Reduced: Wastewater, Ammonia

Process: Equipment Modification

Contact Person: John F. Griffith, (409) 886-6858

2. DESCRIPTION OF PROJECT

Waste aqueous liquid load was reduced by 25,000 pph by installing a larger calandria (reboiler) on an ammonia stripper column.

In the original design of the column, 25%, of the heat input was provided by direct steam injection into the base of the column. The balance of the heat was head transfer through the calandria. Installation of the larger calandria provided for all of the heat input through the calandria which eliminated the direct steam injection. All of the condensate that resulted from the direct steam injection became aqueous liquid waste that had to be disposed of, thus elimination of the direct steam injection eliminated the heat portion of the waste generated.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4 ENVIRONMENTAL BENEFIT

Reduction of 25,000 pph of aqueous liquid waste that is currently disposed of in a deep well disposal system.

5. COST SAVINGS/BENEFIT

The project payback period was 10 years.

Future savings will be realized through reduced investment when facilities are installed to dispose of the aqueous liquid waste by methods other than deep well disposal.

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GCA-Washburn Tunnel Wastewater

Gca1.95

1. GENERAL INFORMATION

 

Location: Pasadena

Number of Employees: 35

Industry: Wastewater Treatment

Waste Reduced: Wastewater

Process: Reuse, Effluent

Contact Person: George Meriwether, (713) 472-5507

2. DESCRIPTION OF PROJECT

The Gulf Coast Authority is a publicly owned waste treatment authority that operates several treatment facilities in the Houston area. The Washburn tunnel facility recently constructed a new belt press station to dewater sludge. The new facility reuses effluent water for belt press process wash, foam control, primary sludge flow control and general plant wash down. Reuse of this water significantly reduces the fresh water requirements of the facility.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

Approximately 530 g.p.m. of plant effluent is used for the belt press with the plant using approximately 800,000 gallons/day.

5. COST SAVINGS/BENEFITS

If this water supply had to be purchased at the rate of $0.0021/gallon, the additional costs to GCA would have bee $613,000 per year. The pumps and associated piping to distribute reuse water plant wide were a small fraction of this amount.

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GCA-Washburn Tunnel-Energy Efficiency

gca2.95

1. GENERAL INFORMATION

 

Location: Pasadena

Number of Employees: 35

Industry: Wastewater Treatment

Waste Reduced: Energy Efficiency

Process: Continuous Monitoring

Contact Person: George Meriwether, (713) 472-5507

2. DESCRIPTION OF PROJECT

The Gulf Coast Authority is a publicly owned waste treatment authority that operates several treatment facilities in the Houston area. To control the electrical cost associated with running aerators, the Washburn tunnel facility installed a continuous Dissolved Oxygen (D.O.) monitoring system. By optimizing the D.O. concentration in the treatment tanks and not continuously running aerators, significant energy savings were achieved.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

The reduced use of aerators not only saves the energy (and the pollutants associated with electrical generation), but also increases the length of service and decrease wastes generated as a result of equipment maintenance.

5. COST SAVINGS/BENEFITS

In 1986, before this system was installed GCA used 1.03 KWhr/# of BOD. In 1994 the rate was 0.86 KWhr/# of BOD. At the 1986 rate this would have cost GCA an additional $270,000 in utility expenditures.

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Go/Dan Industries

godan.92

1. GENERAL INFORMATION

Location: Dallas, Dallas County

Number of Employees:

Industry: Transportation

Waste Reduced: Sludge, Heavy Metals

Process: Wastewater Treatment

Contact Person: M. H. Massey, (214) 637-6740

2. DESCRIPTION OF PROJECT

Wastewater pretreatment system: It is a system for separating precipitated solids from a waste stream. The system consists of primary units, which together remove the heavy metals from a wastewater system.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

The wastewater is collected in the pH adjust tank. When the tank reaches the permissive level, process pumps feed water from the adjust tank through the cells. Ferrous ion is added in the cells. The stream leaving the cell is now essentially a water solution containing metal hydroxides, which can be precipitated from the water. The water is then passed to a retention tank were the solids from the high zinc influent are removed. Polymer is added to overflow from the degassing tank and enters the flash mixing chamber of the Clarifier. From the flash mixing chamber it passes to the flocculating chamber. The liquid flows out through the weir at the top of the Clarifier and is discharged. The slurry transfer pump pulls the solids from the cone of the Clarifier and pumps them to the slurry holding tank. When the slurry holding tank is half full, the filter press system is activated. The slurry pump pumps the solids through the filter press and a thick cake forms in the press. The outflow water from the press is returned to the equalization tank. The solids in the filter press are removed from the press and disposed of by EPA standards.

4. ENVIRONMENTAL BENEFIT

After treatment, results from operating units show heavy metal levels well within EPA specifications.

5. COST SAVINGS/BENEFIT

Purchase and installation cost: $200,000. Approximate annual savings: $60,000.

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Hoechst Celanese

hoechst2.95

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Bishop, Nueces County

Number of Employees: 1.050

Industry: Chemical/Plastics/Pharmaceuticals Manufacturer

Waste Reduced: Multi-Source Leachate (Hazardous)

Process: Landfill Dome

Contact Person: J. Garza, (512) 584-6000

2. DESCRIPTION OF PROJECT

When rain falls into an open hazardous waste landfill, the rainwater percolates through the contents of the landfill cell and is collected via collection headers in the bottom of the landfill. This collected rainwater, also known as multi-source leachate, is classified by environmental regulation as a hazardous waste, and must be managed as such. Before installation of this project, all rainfall (approximately 4.5 million gallons per year) that contacted the material in the Bishop's hazardous waste landfill would be collected and sent to the facilities injection wells for disposal.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

An air-inflated/supported structure (dome) was installed over the Class IH landfill at the Bishop facility to prevent rainfall into and rainwater percolation through the landfill cells. The 85ft. high dome, manufactured by Air Structures American Technologies, Inc. (ASATI), is made of 265,000 square feet of vinyl covered high tensile strength polyester fabric and is inflated by air blowers. The air inside is exchanged and replaced every two hours to facilitate work performed by personnel and equipment inside the dome. When the landfill is full, the dome can be deflated and moved to another location.

4. ENVIRONMENTAL BENEFIT

Installation of this dome prevents rainfall into and rainwater percolation through the landfill cells, thereby eliminating an estimated 4.5 million gallons of hazardous waste generation. This project also extends the life of the landfill by more than 30% since the need for daily capping with wind dispersion material was eliminated upon installation of the dome.

5. COST SAVINGS/BENEFITS

Operating costs avoided by not having to dispose of this leachate in the facilities injection wells are estimated at $60,000 per year.

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Hoechst Celanese- Leachate

hoechst2.95

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Bishop, Nueces County

Number of Employees: 1.050

Industry: Chemical/Plastics/Pharmaceuticals Manufacturer

Waste Reduced: Multi-Source Leachate (Hazardous)

Process: Landfill Dome

Contact Person: J. Garza, (512) 584-6000

2. DESCRIPTION OF PROJECT

When rain falls into an open hazardous waste landfill, the rainwater percolates through the contents of the landfill cell and is collected via collection headers in the bottom of the landfill. This collected rainwater, also known as multi-source leachate, is classified by environmental regulation as a hazardous waste, and must be managed as such. Before installation of this project, all rainfall (approximately 4.5 million gallons per year) that contacted the material in the Bishop's hazardous waste landfill would be collected and sent to the facilities injection wells for disposal.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

 

An air-inflated/supported structure (dome) was installed over the Class IH landfill at the Bishop facility to prevent rainfall into and rainwater percolation through the landfill cells. The 85ft. high dome, manufactured by Air Structures American Technologies, Inc. (ASATI), is made of 265,000 square feet of vinyl covered high tensile strength polyester fabric and is inflated by air blowers. The air inside is exchanged and replaced every two hours to facilitate work performed by personnel and equipment inside the dome. When the landfill is full, the dome can be deflated and moved to another location.

4. ENVIRONMENTAL BENEFIT

Installation of this dome prevents rainfall into and rainwater percolation through the landfill cells, thereby eliminating an estimated 4.5 million gallons of hazardous waste generation. This project also extends the life of the landfill by more than 30% since the need for daily capping with wind dispersion material was eliminated upon installation of the dome.

5. COST SAVINGS/BENEFITS

Operating costs avoided by not having to dispose of this leachate in the facilities injection wells are estimated at $60,000 per year.

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Huntsman Corporation Port Neches

 

 

1. GENERAL INFORMATION

 

Location: Port Neches

Number of Employees: 1,150

Industry: Petrochemicals

Waste Reduced: Wastewater

Process: Wastewater Treatment

Contact Person: Mike Peters, (409) 723-3351

2. DESCRIPTION OF PROJECT

 

Two aerobic digesters were constructed and put in service in June, 1992 for stabilization and reduction of waste activated sludge from our wastewater treatment facility. This process includes tankage, aeration, piping, neutralization and mixing equipment. In the process waste activated sludge is aerated for a period of 20 days, during which time the microorganisms consume their own protoplasm to obtain energy for cell maintenance. The majority of cell tissue is oxidized to carbon dioxide, water and ammonia. The ammonia is oxidized to nitrate as the digestion proceeds.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

4. ENVIRONMENTAL BENEFIT

 

Odors associated with our waste activated sludge have virtually been eliminated. In addition, the quantity of sludge being disposed has been reduced by over 40% or 1.5 million pounds a year.

5. COSTS SAVINGS/BENEFIT

 

Since less sludge needs to be disposed, there is a cost savings of approximately $350,000 per year. The payback period for this project is about 6 years.

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Huntsman

huntsma1.95

1. GENERAL INFORMATION

 

Location: Austin

Number of Employees: 225

Industry: Chemical R&D

Waste Reduced Organics in Wastewater

Process: Supercritical Water Oxidation

Contact Person: Dr. Richard Bennett, (512) 483-0934

2. DESCRIPTION OF PROJECT

Huntsman's research laboratory in Austin generates several organic/water waste streams that were being transported off-site for incineration. Huntsman decided to build the first Super Critical Water Oxidation (SCWO) unit to handle it's waste. Eco Waste Technologies of Austin was contracted to build a 5 g.p.m. unit at the Huntsman facility.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

This is the first commercial application of SCOW. The 5 g.p.m. unit can handle 15-25% organics in water with almost complete conversion (99.95% or higher) to C02 and water. The facility is permitted to discharge water to a publicly owned treatment system, but actual effluent samples from the system have met drinking water standards. Off gas is primarily C02 and water vapor (and N2 from amines) with insignificant concentrations of NO ,X particulates, ozone and ammonia.

4. ENVIRONMENTAL BENEFIT

The Huntsman unit has capacity to treat about 2 million lbs./year of organic by-products from the research facility. The water and gaseous effluent from the process is significantly cleaner than other treatment systems, and it eliminates the potential hazards associated with transporting the material off-site incineration.

5. COST SAVINGS/BENEFITS

The operating costs are projected to be less than $0.20/gallon, once the unit is running at full capacity which will provide significant waste disposal savings to Huntsman.

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Motorola

motor1.94

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Oak Hill Facility, Austin

Number of Employees: 3,500

Industry: Electronics

Waste Reduced: Wastewater, HF

Process: Wastewater Treatment

Contact Person: Curtis Wales, (512) 891-6197

2. DESCRIPTION OF PROJECT

One of the key process steps in all semiconductor manufacturing is the etching of the wafer. Etching refers to the process of removing materials in specified areas which leaves minute and intricate patterns on the wafer thereby making a semiconductor. The chemical predominately used in this industry for etching is Hydrofluoric Acid (HF). HF is a very hazardous waste and requires a great deal of care to manage and dispose of it property. In 1992 Motorola generated over 680 tons of HF waste which in the past was disposed of by deep well injection. In June of 1992 the Motorola Oak Hill facility installed a Fluoride Waste Treatment System on site to completely neutralize this very hazardous stream. The treatment method for our system is a one step chemical reaction of mixing the HF waste and Calcium Hydroxide, or Lime as it is commonly known, together which neutralizes the acid and balances the pH at the same time. It forms calcium fluoride, a stable, non hazardous, and very harmless material.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

In 1993, Motorola expanded the FWTS to keep up with increased HF usage. The expansion increased our neutralization time and equipment efficiency by allowing us to filter one of our two reaction tanks while we are doing a reaction in the other. It also has almost doubled our capacity to treat HF waste.

4. ENVIRONMENTAL BENEFIT

The benefits for the Flouride Waste Treatment are:

1. The on site treatment system keeps this very hazardous waste from traveling on our public highways to disposal sites in different areas. It is completely contained in covered tanks and continuously monitored for correct operation. All of these benefits represent an extensive reduction of potential impact to human health and the environment.

2. The FWTS also represents a real waste minimization effort which will account for a 46% reduction of Motorola's TOTAL hazardous waste generation and a 99% reduction of our HF waste generation.

3. This sytem could be used industry wide for semiconductor plants.

176

5. COST SAVINGS/BENEFIT

Motorola spent $378,00 for the initial unit and an additional $160,000 on the expansion to keep up with increases in production. A cost savings of over $24,000 for 1992 was determined by comparing the $0.44/gal cost to deepwell with the $0.29/gal cost to operate the FWTS.

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Oxy Petrochemicals, Inc.

oxycc 1.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Corpus Christi, Nueces County

Number of Employees: 310

Industry: Chemicals. Organic

Waste Reduced: Waste Water, Copper

Process: Wastewater Treatment

Contact Person: Michael Mudrock, (512) 242-8098

2. PROJECT DESCRIPTION

In 1991, a copper discharge limitation was added to the facility's wastewater permit. An initial analysis of the wastewater showed the levels of copper present were much higher than permitted. OxyChem determined that the plant water supplier (City of Corpus Christi) was dosing the water with copper sulfate for algae control.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

OxyChem and the City of Corpus Christi Water Department worked together over a period of more than eight months during 1992 to determine copper removal/alternative treatment methods and implement a solution. Both parties contributed research efforts. Analytical services to monitor copper releases at the City's treatment plant were provided by OxyChem. Chlorine dioxide and potassium permanganate were identified and evaluated as substitutes for the copper sulfate. In September 1992, the City of Corpus Christi began utilizing the alternative algicide treatment in lieu of the copper sulfate.

4. ENVIRONMENTAL BENEFIT

The substitution source reduced copper from not only OxyChem's water but other industrial customers of the City of Corpus Christi. Total copper releases to the environment were reduced.

5. COST SAVINGS/BENEFIT

OxyChem avoided the expense of designing, installing and operating a water pretreatment facility for its process water. In addition, the water for copper removal would have created additional solid waste.

TOP


Phillips Petroleum Company

phillip1.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Sweeny

Number of Employees: 1,459

Industry: Petroleum Refining

Waste Reduced: Wastewater

Process: Wastewater Treatment

Contact Person: Dan Hunter, (409) 491-2200 ext 2216

2. DESCRIPTION OF PROJECT

Phillips Petroleum has constructed an artificial marsh to study the removal of organic chemical waste, heavy metals and toxicity. The test facility consists of two parallel channels of rooted and floating aquatic vegetation with design treatment capacities ranging from 20,000 gpd to 100,000 gpd. Cattails and bulrush are contained in one of the channels. The other was planted with duckweed and torpedo grass. However, the torpedo grass was overtaken by the adjacent cattails, and our attempt at growing duckweed was unsuccessful. Additional floating aquatic plants are still being researched, while testing continues on the channels containing rooted aquatic plants.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

The purpose of this project is to evaluate the potential of various aquatic plants for treating organic chemical wastewater. Taking advantage of this new technology could result in cleaner discharge at a lower cost than the traditional wastewater treatment facility. Biotech Industries and Dr. B.C. Wolverton of Wolverton Environmental Services are providing scientific and engineering design services.

4. ENVIRONMENTAL BENEFIT

Phillips has found that the pilot artificial marsh is capable of reducing BOD by 61 % and NH3-N by 32%. Test results also show reductions in the concentration of oil, suspended solids and chromium. Detected increases in phenol may indicate the breakdown of certain aromatic compounds. Significant reductions in toxicity measured with a microtox are also consistently observed.

5. COST SAVINGS/BENEFIT

An artificial marsh requires less energy and is less costly to operate than traditional mechanical treatment systems.

TOP


Rhone Poulenc

rhonep11.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Houston, Harris County

Number of Employees: 189

Industry: Chemicals, Inorganic

Waste Reduced: Wastewater, Copper

Process: Wastewater Treatment, Sulfide Precipetation

Contact Person: George Ramsay, (713) 928-3411 ext. 1485

2. DESCRIPTION OF THE PROJECT

Last year the limit for copper in our NPDES effluent was reduced from a daily average of 0.83 Ib/day to 0.11 lb/day. The daily maximum was reduced from 1.37 lb/day to 0.11 lb/day. The concentration of copper in the discharge now could not exceed 10 to 15 ppb, depending on the flowrate. Much of the copper in the effluent comes from corrosion of copper alloy heat exchangers, even though the corrosion is low (0.1 mils per year). The copper in the effluent was being removed by hydroxide precipitation in settling ponds.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

Sulfide-based precipitation was selected for removing the copper. Retubing with stainless steel would be very expensive and would reduce the heat transfer of the heat exchangers. Hydroxide precipitation could not reduce the copper to less than about 20 ppb.

Sodium sulfide and dithiocarbamate were ruled out because of their known toxicity to our biomonitoring species M,, sepsis bahia (grass shrimp). Dithiocarbamate attached to insoluble starch was non-toxic to the shrimp in laboratory tests but seemed to decompose to toxic compounds in the ponds, possibly due to sun light. Trisodium trimercapto-triazine was non-toxic in field tests but at times was difficult to flocculate. A proprietary sulfide-based precipitant called MR-3300 was found to be non-toxic and reduces the copper to 1 to 10 ppb. By using filtration in addition to clarification lower copper concentrations are expected. The MR-3300 is sold by Southern Water Treatment, located in Greenville, South Carolina.

4. ENVIRONMENTAL BENEFIT

Reducing the copper in our effluent is expected to improve the environmental quality of the Galveston Bay.

 

5. COST SAVINGS/BENEFIT

 

Meeting the new copper limit increases our costs by $50,000 to $60,000 per year.

TOP 


Motorola-Hydrofluoric Acid

motor1.94

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Oak Hill Facility, Austin

Number of Employees: 3,500

Industry: Electronics

Waste Reduced: Wastewater, HF

Process: Wastewater Treatment

Contact Person: Curtis Wales, (512) 891-6197

2. DESCRIPTION OF PROJECT

One of the key process steps in all semiconductor manufacturing is the etching of the wafer. Etching refers to the process of removing materials in specified areas which leaves minute and intricate patterns on the wafer thereby making a semiconductor. The chemical predominately used in this industry for etching is Hydrofluoric Acid (HF). HF is a very hazardous waste and requires a great deal of care to manage and dispose of it property. In 1992 Motorola generated over 680 tons of HF waste which in the past was disposed of by deep well injection. In June of 1992 the Motorola Oak Hill facility installed a Fluoride Waste Treatment System on site to completely neutralize this very hazardous stream. The treatment method for our system is a one step chemical reaction of mixing the HF waste and Calcium Hydroxide, or Lime as it is commonly known, together which neutralizes the acid and balances the pH at the same time. It forms calcium fluoride, a stable, non hazardous, and very harmless material.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

In 1993, Motorola expanded the FWTS to keep up with increased HF usage. The expansion increased our neutralization time and equipment efficiency by allowing us to filter one of our two reaction tanks while we are doing a reaction in the other. It also has almost doubled our capacity to treat HF waste.

4. ENVIRONMENTAL BENEFIT

The benefits for the Flouride Waste Treatment are:

1. The on site treatment system keeps this very hazardous waste from traveling on our public highways to disposal sites in different areas. It is completely contained in covered tanks and continuously monitored for correct operation. All of these benefits represent an extensive reduction of potential impact to human health and the environment.

2. The FWTS also represents a real waste minimization effort which will account for a 46% reduction of Motorola's TOTAL hazardous waste generation and a 99% reduction of our HF waste generation.

3. This sytem could be used industry wide for semiconductor plants.

176

5. COST SAVINGS/BENEFIT

Motorola spent $378,00 for the initial unit and an additional $160,000 on the expansion to keep up with increases in production. A cost savings of over $24,000 for 1992 was determined by comparing the $0.44/gal cost to deepwell with the $0.29/gal cost to operate the FWTS.

TOP


Oxy Petrochemicals, Inc.-Copper

oxycc 1.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Corpus Christi, Nueces County

Number of Employees: 310

Industry: Chemicals. Organic

Waste Reduced: Waste Water, Copper

Process: Wastewater Treatment

Contact Person: Michael Mudrock, (512) 242-8098

2. PROJECT DESCRIPTION

In 1991, a copper discharge limitation was added to the facility's wastewater permit. An initial analysis of the wastewater showed the levels of copper present were much higher than permitted. OxyChem determined that the plant water supplier (City of Corpus Christi) was dosing the water with copper sulfate for algae control.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

OxyChem and the City of Corpus Christi Water Department worked together over a period of more than eight months during 1992 to determine copper removal/alternative treatment methods and implement a solution. Both parties contributed research efforts. Analytical services to monitor copper releases at the City's treatment plant were provided by OxyChem. Chlorine dioxide and potassium permanganate were identified and evaluated as substitutes for the copper sulfate. In September 1992, the City of Corpus Christi began utilizing the alternative algicide treatment in lieu of the copper sulfate.

4. ENVIRONMENTAL BENEFIT

The substitution source reduced copper from not only OxyChem's water but other industrial customers of the City of Corpus Christi. Total copper releases to the environment were reduced.

5. COST SAVINGS/BENEFIT

OxyChem avoided the expense of designing, installing and operating a water pretreatment facility for its process water. In addition, the water for copper removal would have created additional solid waste.

TOP


Phillips Petroleum Company-Artificial Marsh

phillip1.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Sweeny

Number of Employees: 1,459

Industry: Petroleum Refining

Waste Reduced: Wastewater

Process: Wastewater Treatment

Contact Person: Dan Hunter, (409) 491-2200 ext 2216

2. DESCRIPTION OF PROJECT

Phillips Petroleum has constructed an artificial marsh to study the removal of organic chemical waste, heavy metals and toxicity. The test facility consists of two parallel channels of rooted and floating aquatic vegetation with design treatment capacities ranging from 20,000 gpd to 100,000 gpd. Cattails and bulrush are contained in one of the channels. The other was planted with duckweed and torpedo grass. However, the torpedo grass was overtaken by the adjacent cattails, and our attempt at growing duckweed was unsuccessful. Additional floating aquatic plants are still being researched, while testing continues on the channels containing rooted aquatic plants.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

The purpose of this project is to evaluate the potential of various aquatic plants for treating organic chemical wastewater. Taking advantage of this new technology could result in cleaner discharge at a lower cost than the traditional wastewater treatment facility. Biotech Industries and Dr. B.C. Wolverton of Wolverton Environmental Services are providing scientific and engineering design services.

4. ENVIRONMENTAL BENEFIT

Phillips has found that the pilot artificial marsh is capable of reducing BOD by 61 % and NH3-N by 32%. Test results also show reductions in the concentration of oil, suspended solids and chromium. Detected increases in phenol may indicate the breakdown of certain aromatic compounds. Significant reductions in toxicity measured with a microtox are also consistently observed.

5. COST SAVINGS/BENEFIT

An artificial marsh requires less energy and is less costly to operate than traditional mechanical treatment systems.

TOP


 

Rhone Poulenc-Copper

rhonep11.93

1. GENERAL INFORMATION CLEAN INDUSTRIES 2000 Member

 

Location: Houston, Harris County

Number of Employees: 189

Industry: Chemicals, Inorganic

Waste Reduced: Wastewater, Copper

Process: Wastewater Treatment, Sulfide Precipetation

Contact Person: George Ramsay, (713) 928-3411 ext. 1485

2. DESCRIPTION OF THE PROJECT

Last year the limit for copper in our NPDES effluent was reduced from a daily average of 0.83 Ib/day to 0.11 lb/day. The daily maximum was reduced from 1.37 lb/day to 0.11 lb/day. The concentration of copper in the discharge now could not exceed 10 to 15 ppb, depending on the flowrate. Much of the copper in the effluent comes from corrosion of copper alloy heat exchangers, even though the corrosion is low (0.1 mils per year). The copper in the effluent was being removed by hydroxide precipitation in settling ponds.

3. INNOVATIVE APPLICATION OF TECHNOLOGY

Sulfide-based precipitation was selected for removing the copper. Retubing with stainless steel would be very expensive and would reduce the heat transfer of the heat exchangers. Hydroxide precipitation could not reduce the copper to less than about 20 ppb.

Sodium sulfide and dithiocarbamate were ruled out because of their known toxicity to our biomonitoring species M,, sepsis bahia (grass shrimp). Dithiocarbamate attached to insoluble starch was non-toxic to the shrimp in laboratory tests but seemed to decompose to toxic compounds in the ponds, possibly due to sun light. Trisodium trimercapto-triazine was non-toxic in field tests but at times was difficult to flocculate. A proprietary sulfide-based precipitant called MR-3300 was found to be non-toxic and reduces the copper to 1 to 10 ppb. By using filtration in addition to clarification lower copper concentrations are expected. The MR-3300 is sold by Southern Water Treatment, located in Greenville, South Carolina.

4. ENVIRONMENTAL BENEFIT

Reducing the copper in our effluent is expected to improve the environmental quality of the Galveston Bay.

 

5. COST SAVINGS/BENEFIT

 

Meeting the new copper limit increases our costs by $50,000 to $60,000 per year.

TOP